000 -LEADER |
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02950nam a22004455i 4500 |
003 - CONTROL NUMBER IDENTIFIER |
control field |
OSt |
005 - DATE AND TIME OF LATEST TRANSACTION |
control field |
20140310153328.0 |
007 - PHYSICAL DESCRIPTION FIXED FIELD--GENERAL INFORMATION |
fixed length control field |
cr nn 008mamaa |
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
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130809s2013 gw | s |||| 0|eng d |
020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
International Standard Book Number |
9783319011349 |
|
978-3-319-01134-9 |
050 #4 - LIBRARY OF CONGRESS CALL NUMBER |
Classification number |
QD415-436 |
082 04 - DEWEY DECIMAL CLASSIFICATION NUMBER |
Classification number |
547 |
Edition number |
23 |
264 #1 - |
-- |
Cham : |
-- |
Springer International Publishing : |
-- |
Imprint: Springer, |
-- |
2013. |
912 ## - |
-- |
ZDB-2-CMS |
100 1# - MAIN ENTRY--PERSONAL NAME |
Personal name |
Lennox, Alastair J. J. |
Relator term |
author. |
245 10 - IMMEDIATE SOURCE OF ACQUISITION NOTE |
Title |
Organotrifluoroborate Preparation, Coupling and Hydrolysis |
Medium |
[electronic resource] / |
Statement of responsibility, etc |
by Alastair J. J. Lennox. |
300 ## - PHYSICAL DESCRIPTION |
Extent |
XV, 223 p. 308 illus., 96 illus. in color. |
Other physical details |
online resource. |
440 1# - SERIES STATEMENT/ADDED ENTRY--TITLE |
Title |
Springer Theses, Recognizing Outstanding Ph.D. Research, |
International Standard Serial Number |
2190-5053 |
505 0# - FORMATTED CONTENTS NOTE |
Formatted contents note |
General Introduction -- Organotrifluoroborate Preparation -- Organotrifluoroborate Coupling -- Organotrifluoroborate Hydrolysis -- Conclusions and Future Work -- Experimental: General Experimental Details -- Experimental: Organotrifluoroborate Preparation -- Experimental: Organotrifluoroborate Coupling -- Experimental: Organotrifluoroborate Hydrolysis. |
520 ## - SUMMARY, ETC. |
Summary, etc |
Alistair Lennox's thesis reports on the reactivity of organotrifluoroborates, which are becoming increasingly important reagents in synthesis. The thesis is divided into three sections. The first section describes a method for preparing organotrifluoroborates. The second section reports on a mechanistic investigation into the main application of RBF3K reagents as coupling partners in Suzuki-Miyaura coupling, phenomena identified as arising from organotrifluoroborate hydrolysis and fluoride release. The final section reports on a detailed investigation into the hydrolysis mechanism, a prerequisite for their Suzuki-Miyaura coupling, and how it may be predicted and controlled. This research has uncovered many interesting and useful details and shows how problems associated with Suzuki-Miyaura coupling can best be addressed. There has already been wide industrial uptake of the new procedures and insights. The broad nature and clear and succinct style will make the thesis a valuable resource for anyone working in synthesis, organometallic chemistry, or in homogeneous catalysis. |
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
Topical term or geographic name as entry element |
Chemistry. |
|
Topical term or geographic name as entry element |
Chemistry, Organic. |
|
Topical term or geographic name as entry element |
Chemical engineering. |
|
Topical term or geographic name as entry element |
Catalysis. |
|
Topical term or geographic name as entry element |
Chemistry. |
|
Topical term or geographic name as entry element |
Organic Chemistry. |
|
Topical term or geographic name as entry element |
Catalysis. |
|
Topical term or geographic name as entry element |
Industrial Chemistry/Chemical Engineering. |
710 2# - ADDED ENTRY--CORPORATE NAME |
Corporate name or jurisdiction name as entry element |
SpringerLink (Online service) |
773 0# - HOST ITEM ENTRY |
Title |
Springer eBooks |
776 08 - ADDITIONAL PHYSICAL FORM ENTRY |
Display text |
Printed edition: |
International Standard Book Number |
9783319011332 |
856 40 - ELECTRONIC LOCATION AND ACCESS |
Uniform Resource Identifier |
http://dx.doi.org/10.1007/978-3-319-01134-9 |
942 ## - ADDED ENTRY ELEMENTS (KOHA) |
Source of classification or shelving scheme |
|
Item type |
E-Book |